“Spectra taken of fibres from a garment can exhibit some variation...This may be because the dye has been taken up differently (such as in cotton fibres) or perhaps because the outermost fibres have been bleached more by sunlight in comparison to those from deeper within the fabric.... The criteria for comparing fibres to the reference population are that for a recovered fibre the spectrum should fall within the variation observed in the reference fibres. Whilst there are always areas within a reference sample that vary, there are also areas of the spectra which display a high level of consistency – such as the position of the lamda max [the wavelength at which the fibre exhibits its maximum absorbance]. When interpreting spectral matches, the entire spectrum is observed, with particular attention given to regions of the recovered fibre where the reference displays a high level of consistency. If the [recovered] fibre displays a feature in the[se] regions which has not been demonstrated in the reference population (for example, increasing in slope where the reference fibres decrease) then it is distinguished from the reference.”
“...it can be seen that they [Boydlands and Snowcroft fibres] are subtly, but consistently, different. Some differences are present on the raw data plot (see appendix figure 13) but more are obvious on the first derivative plot (see appendix figure 14)........With the exception of one flock fibre recovered from the fence post, all of the flock fibres recovered from 15 Boydlands were distinguishable from those recovered at 8 Snowcroft. In my opinion, the findings provide no support for the prosecution that the flock fibres...arose from the same source....As a single flock fibre indistinguishable from those found at 8 Snowcroft could have been transferred to the fence post via contacts other than a direct contact, I am reluctant to attach any weight to its finding.”
“Does the variation in morphology and results of instrumental analysis of the fibres in each population fall within the same observable limits or are they incongruent in that respect?”
“The fibres in each population are dark (black) in colour to the naked eye but appear almost purple under high power microscopy. I can confirm they are flocked and are derived from nylon fibres. I can confirm there is a variation [with]in each population in terms of the fibre diameter, delustrant concentration, morphology and colour intensity of each population; however, the range and degree of this variation is congruent between each population.”
“A range of fibre samples was measured using J&M MSP400 and J&M MSP800 microspectrophotometers across the visible and UV/visible wavelength ranges respectively. The first derivative of the absorbance spectra was then calculated and studied. When the absorbance spectra produced for some samples were broad and featureless, the first derivative spectra provided more points of comparison that facilitated discrimination. For many of the samples, calculating the first derivative did not result in any additional discrimination due to the high number of points of comparison present in the absorbance spectra. However, for the samples that exhibited a high level of intra-sample colour variation (e.g. through uneven uptake common in cotton and wool, etc.) which was evident in the absorbance spectra, the associated first derivative spectra highlighted this variation between the fibres and could potentially have resulted in false exclusions. The results show that whilst calculating first derivative can be a useful aid in the comparison of spectra, a high degree of caution is required when applying this method to fibres which exhibit large intra-sample variation in colour.”
“In summary, TLC separates the dyes used in fibres. However, it does not inform as to the relative concentrations of individual dyes. For illustration purposes only, if a fibre from one scene is dyed with 50% dye A, 26% dye B and 24% dye C, a TLC plate will probably show three spots in three different positions on the plate. Another fibre from another scene but dyed with 50% dye A, 24% dye B and 26% dye C will also provide the same three spots in the same positions. It will be impossible to tell them apart by TLC – even though the dye combinations will be different.”
“My observations [at Contact Traces] tended to confirm what I had already observed using the FSS microscope, namely that there was a range of dye intensity, fibre diameter and levels of delustrant common to both populations. The variation in physical characteristics was typical of that expected from flock fibres. I had, however, some concerns over a subtle, yet consistent, difference in fluorescence between the populations which I believe was more easily observed using Mr Coyle’s microscope than that I had used at the FSS. I also understand that both parties have observed what appears to be a greater quantity of thicker, darker flock fibres at the crime scene and some of the flock fibres at the scene appear with the gluing agent intact... Since the release of Mr Coyle’s statements the FSS has had the opportunity to review his work and, as a consequence of the challenge, they have performed a considerable amount of extra work to understand matters of discrepancy for themselves... As a result...Mr Palmer has rebutted two main aspects of that of Mr Coyle’s, namely whether the variation in fluorescence is sufficiently significant to discriminate between the two populations, and whether the application of the first derivative to black nylon flock fibres is a safe test for elimination purposes. I have read Mr Coyle’s response, dated11 March 2010 in which he appears to stand by his initial findings.”
“The FSS Microscope Comparison Method: a scientist examines a sub-sample of the population from or connected with a potential source – in this case the suspect’s house – noting the range of physical characteristics. S/he then takes sub-samples of fibres from various locations at the crime scene, again taking note of the range of physical characteristics. By doing so s/he builds up a memory bank of the range. They then go on to compare directly a quantity of the fibres and take the range of characteristics into account. All positive findings are then checked by a second scientist and any disputes resolved by a third scientist acting as arbitrator – usually another reporting scientist. The Contact Traces Microscope Comparison Method: after sub-sampling from various areas related to the scene and comparing the samples to each other the examiner builds up a catalogue of the range. The examiner then takes sub-samples from the suspect’s environment and duplicates the process. Finally, both populations are systematically compared; each fibre from one sample being compared with each fibre from the other. A fibre is excluded if it does not share very similar physical characteristics. A second scientist then checks the positive findings and further eliminates any individual fibres if s/he considers one to be different. There is no third adjudicator and any discrepancies are automatically eliminated. Therefore, only the very best of matches remain.”
“In my opinion, there are various mechanisms and degrees of contact that could lead to the sort of subtle differences between the two populations of black flock fibres in this case. For instance, it is perfectly feasible to propose that the greater number of thicker fibres at the scene could have been transferred as a result of increased levels of contact through a struggle and/or the moving of the deceased’s body. This would be supported by the observation of occasionally finding the gluing agent still to be intact on fibres at the crime scene.”
“...I consider the black nylon flock fibres in question to be unusual source of fibres for examination in a forensic laboratory. The range observed in both populations is complex, more so in that observed at the crime scene. It is important to recognise that this is not a simple case of assessing whether the fibres match or not. Without the garment(s) as reference, this comparison and its evaluation was never going to be easy and remains open to challenge. I believe it to be unlikely that the comparison microscope used by FSS at the original trial, which probably reflected the technology then, would have had the capability to detect the subtle differences in fluorescence in as much detail.”
“I am in agreement that there are some differences between the two fibre populations. I am in disagreement with Mr Coyle that these differences are sufficient on their own to exclude an association between the populations.”
“Whilst the fibres from the different areas at 15 Boydlands were deemed indistinguishable from each other, they were different when compared to those fibres recovered from 8 Snowcroft with the exception of one fibre found on the floor of bedroom 3 (Rec number 196, NAM52, slide 1, number 4). This fibre was indistinguishable from one of the types of carbon black pigmented polyester fibres observed. However, in my opinion modern forensic fibre analysis techniques are unable [to] discriminate carbon black pigmented fibres to a high level, and this, together with their widespread use as a cheap way of producing black fibres, makes carbon black pigmented fibres poor value as a target fibre. Any links based on carbon black pigmented fibres should be treated with a high degree of caution.”
“...given the black polyester fibres were recovered, in particular, from the deceased’s skin in the same location as that of the nylon flock then it is reasonable to suggest that even if they did originate from more than one garment they were transferred together and at the same time. As such the findings may be considered in association to each other. Furthermore, if it is assumed that the black polyester fibres have originated from the same source as the black nylon flock fibres, as proposed by Mr Coyle, then the additional presence of two types of black polyester, in my opinion, provides further support for the assertion that the nylon flock fibres recovered from Simon Hall’s wardrobe are associated with those recovered from the body of Joan Albert. Either way, in my opinion, the presence of three fibre collectives recovered from the body of Joan Albert and the wardrobe of Simon Hall provides strong scientific support for the assertion that the fibres are associated with each other and have originated from a similar source or sources.”
“I am not persuaded that the House laid down any incorrect principle in Stafford, so long as the Court of Appeal bears very clearly in mind that the question for its consideration is whether the conviction is safe and not whether the accused is guilty … The Court of Appeal can make its assessment of the fresh evidence it has heard, but save in a clear case it is at a disadvantage in seeking to relate that evidence to the rest of the evidence which the jury heard. For these reasons it will usually be wise for the Court of Appeal, in a case of any difficulty, to test their own provisional view by asking whether the evidence, if given at the trial, might reasonably have affected the decision of the trial jury to convict. If it might, the conviction must be thought to be unsafe.”
“11...The judgment in “fresh evidence” cases will inevitably therefore continue to focus on the facts before the trial jury, in order to ensure that the right question - the safety, or otherwise, of the conviction - is answered. It is integral to [that] process that if the fresh evidence is disputed, this Court must decide whether and to what extent it should be accepted or rejected, and if it is to be accepted, to evaluate its importance, or otherwise, relative to the remaining material which was before the trial jury: hence the jury impact test. Indeed, although the question did not arise in Pendleton, the fresh evidence produced by the appellant, or indeed the Crown, may serve to confirm rather than undermine the safety of the conviction. Unless this evaluation is carried out, it is difficult to see how this Court can carry out its statutory responsibility in a fresh evidence case, and exercise its “powers of review to guard against the possibility of injustice”
“Again, I feel it is necessary to record that I find it particularly unusual to observe two credible forensic examiners disagreeing on the outcome of a microscopic comparison in that, in basic terms, the FSS say the black polyester fibres match, whilst Contact Traces say they don’t. This appears to mirror, in part, the outcome of the comparison of nylon flock fibres which play a key role in this case. This discrepancy is an area of particular concern. I can only suggest, on reflection, of the science involved, this has occurred as a result of differing operational procedures and/or reporting guidelines.”
“As both the flock fibres and the carbon black polyester fibres are present on the body and at the points of entry, the most likely explanation for the presence of these fibres is that they were transferred as a result of contact between the offender and the scene.”